Isopropyl chloroformate → HCID 67616408, compound

HRID 1468012Notes

Reaction equation

[NH:1]1[C:9]2[C:4](=[CH:5][C:6]([NH2:10])=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[CH:11]([O:14][C:15](Cl)=[O:16])([CH3:13])[CH3:12]>>[NH:1]1[C:9]2[C:4](=[CH:5][C:6]([NH:10][C:15](=[O:16])[O:14][CH:11]([CH3:13])[CH3:12])=[CH:7][CH:8]=2)[CH:3]=[CH:2]1

Participants

Reactant 2

HCID 7917Isopropyl chloroformate

HCID 788675-Aminoindole

Product 1

HCID 67616408HCID 67616408, compound

Procedure

The title compound was prepared by following the similar procedure as described in Intermediate-52, using 1H-indol-5-amine and isopropyl-chloro-formate (0.72 g, 52%); MS: 219(M+1).

Sources & evidence

ORD record: ord-3f89f7e2f58e466a862edadd1301d2d7
Source dataset: uspto-grants-2015_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09000175B2

Reaction notes

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