1,2,3,4-Tetramethylbenzene → HCID 86689400, compound

HRID 1468557Notes

Reaction equation

HRID 1468557 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[C:4]([CH3:9])[C:3]=1[CH3:10].[Cl-:11].[Cl-].[Cl-].[Cl-].[Zr+4:15]>C1(C)C=CC=CC=1>[Cl-:11].[Cl-:11].[Cl-:11].[Cl-:11].[Zr+4:15].[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[C:4]([CH3:9])[C:3]=1[CH3:10]

Participants

4

Reactant 2

HCID 102631,2,3,4-TetramethylbenzeneHCID 9856075Zirconium chloride (ZrCl4), (T-4)-

Product 1

HCID 86689400HCID 86689400, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

0.71 g (5.29 mmol) of tetramethylbenzene is dissolved in 80 mL of toluene. 2.49 g (10.69 mmol) of zirconium tetrachloride is added using a Bush tube.

Sources & evidence

ORD record
ord-3fe68a91ada44e9fb7be03726272ded3
Source dataset
uspto-grants-2015_04
Patent number
US09005556B2

Reaction notes

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