HCID 19385238, compound → HCID 70982806, compound

HRID 1468691Notes

Reaction equation

HRID 1468691 reaction equation
[CH:1]1([C:4]2[S:5][C:6]3[CH:12]=[C:11]([O:13]C)[C:10]([CH3:15])=[CH:9][C:7]=3[N:8]=2)[CH2:3][CH2:2]1.[Br:16]C1C2SC=NC=2C=C(C)C=1O.COC1C(C)=CC2N=CSC=2C=1>>[Br:16][C:12]1[C:6]2[S:5][C:4]([CH:1]3[CH2:3][CH2:2]3)=[N:8][C:7]=2[CH:9]=[C:10]([CH3:15])[C:11]=1[OH:13]

Participants

4

Reactant 3

HCID 19385238HCID 19385238, compoundHCID 70981708HCID 70981708, compoundHCID 71003635HCID 71003635, compound

Product 1

HCID 70982806HCID 70982806, compound

Procedure

Compound 15 was prepared from compound 6B by the method used to prepare compound 5D from compound 5B as outlined in Example 1. LCMS-ESI+: calc'd for C141H10BrNOS: 284.0 (M+H+). Found: 284.2 (M+H+).

Sources & evidence

ORD record
ord-5b41d501425e4b27b8272a099ccbe571
Source dataset
uspto-grants-2015_04
Patent number
US09006229B2

Reaction notes

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