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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1468832Generated: November 1, 2026

Bromide ion → (4-(Bromomethyl)-2,6-difluorophenyl)(methyl)sulfane

https://huagongshe.com/reaction/1468832

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBromide ionHCID 259—
Reactant(3,5-Difluoro-4-(methylthio)phenyl)methanolHCID 22746033—
Reactant3,5-Difluoro-4-(methylthio)benzaldehydeHCID 22746682—
Product(4-(Bromomethyl)-2,6-difluorophenyl)(methyl)sulfaneHCID 22746076—

Reaction Steps

The product from step B was converted to the bromide according to the procedure from intermediate 5 (step A). 1H NMR (500 MHz, CDCl3) δ 7.36 (d, J 7.5 Hz, 2H), 4.82 (s, 2H), 2.88 (s, 3H)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09006228B2
Source datasetuspto-grants-2015_04
ORD IDord-cb7a942a440047ad92464ae810f12cb4
Source noteuspto-grants-2015_04