Potassium Carbonate → HCID 71678380, compound

Participants

Reaction Steps

The title compound was prepared following the procedure described in Intermediate-11, step-3 using 4-chloro-8-nitroquinoline (Intermediate-11, step-2, 200 mg, 0.96 mmol), 4-(trifluoromethyl)phenol (233 mg, 1.43 mmol), K2CO3 (264 mg, 1.91 mmol) in CH3CN (5 mL) to afford 200 mg of the title product. 1H NMR (300 MHz, DMSO d6): δ 8.85 (d, J=4.8 Hz, 1H), 8.56 (d, J=8.4 Hz, 1H), 8.36 (d, J=7.2 Hz, 1H), 7.93 (d, J=8.7 Hz, 2H), 7.82 (t, J=8.1 Hz, 1H), 7.58 (d, J=8.4 Hz, 2H), 6.98 (d, J=5.4 Hz, 1H).

Provenance & Evidence