HRID1470390
反应详情
EQUATION
反应方程式
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反应物
PRODUCTS
产物
PROCEDURE
实验过程
The compound was synthesized according to the procedure L with 3-[2-(3,4-dimethoxyphenyl)furo[3,2-b]pyridin-7-yl]-2-methylaniline (40.00 mg, 0.11 mmol) and 4,5,6,7-tetrahydro-1-benzothiophene-2-carbonyl chloride (24.5 mg, 0.12 mmol) and N-ethyl-N-isopropylpropan-2-amine (0.03 ml, 0.17 mmol). The title compound was obtained as a yellow solid (32 mg, 55%). HPLC (method F): 96%, RT=4.512 min. 1H NMR (DMSO-d6) δ [ppm] 9.95 (s, 1H), 8.53 (d, 1H), 7.63 (d, 2H), 7.45-7.27 (m, 6H), 7.03 (d, 1H), 3.83 (s, 3H), 3.76 (s, 3H), 2.70 (s, 2H), 2.55 (m, 2H), 2.05 (s, 3H), 1.72-1.69 (m, 4H). MS: m/z=525 [M+H]+, RT=4.50 min.
WORKUP
后处理
- customThe compound was synthesized