HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-1-nitro-4-propoxybenzene → 2-Methoxy-4-propoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-1-nitro-4-propoxybenzene | HCID 67125447 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-Methoxy-4-propoxyaniline | HCID 63677805 | — |
Reaction Steps
1.40 g (6.63 mmol) 2-Methoxy-1-nitro-4-propoxybenzene in 20 mL EtOAc is charged with 100 mg Pd/C (5%) and hydrogenated at rt with a hydrogen pressure of 50 psi. The mixture is filtered and the solvent is removed in vacuo. The crude product is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09006450B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-6715a7cc079b4e02b2b5dfba75a055d9 |
| Source note | uspto-grants-2015_04 |