Ethanol → HCID 73438578, compound

Participants

Reaction Steps

To a solution of the above obtained solution of 2-amino-3,5-dichloro-N-(bis-2-propyl-λ4-sulfanylidene)benzamide (6.7 mL; ˜3.6 mmol) was added potassium carbonate (0.60 g, 4.3 mmol, 1.20 equiv) and a solution of 2-(3-chloro-2-pyridyl)-5-(trifluoromethyl)pyrazole-3-carbonyl chloride (1.34 g, 4.31 mmol, 1.20 equiv.) in toluene (10 mL) at room temperature. After 6 h at this temperature, the mixture poured onto water and treated with a small amount of ethanol under sonification. The resulting precipitate was collected by filtration, washed with water and diisopropyl ether and dried to obtain the title compound (1.29 g, 60%).

Provenance & Evidence