HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrodiphenylamine → N-Phenyl-o-phenylenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrodiphenylamine | HCID 8407 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-Phenyl-o-phenylenediamine | HCID 68297 | — |
Reaction Steps
To a pressure reaction bottle was added 10 g 2-nitrodiphenylamine, 0.5 g 5% palladium on carbon and 100 ml 95% ethanol. The mixture was hydrogenated at 22 C and 40 psi hydrogen for 2 hours. Following filtration through celite and solvent removal, an oil was obtained that crystallized on standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09011734B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-543b69b6cf424f5ba71a793caa3e2fec |
| Source note | uspto-grants-2015_04 |