反应详情

To a pressure reaction bottle were added 1.6 g 2-(benzyloxy)-6-butylpyridine, 0.2 g 5% palladium on carbon and 50 ml ethanol. The mixture was hydrogenated at 22 C and 40 psi hydrogen for 16 hours. Following filtration through celite and solvent removal, an oil was obtained that crystallized on standing to give 0.9 g.

1. customTo a pressure reaction bottle
2. filtrationfiltration through celite and
3. customsolvent removal
4. customan oil was obtained
5. customthat crystallized
6. customto give 0.9 g