HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Bis(trifluoromethyl)phenol → Tetrabutylammonium 3,5-Bis(trifluoromethyl)phenoxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Bis(trifluoromethyl)phenol | HCID 67680 | — |
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Tetrabutylammonium 3,5-Bis(trifluoromethyl)phenoxide | HCID 86619914 | — |
Reaction Steps
To a flask were added 1.0 g 3,5-bis(trifluoromethyl)phenol, 1.8 g of a 55-60% solution of tetrabutylammonium hydroxide in water and 10 ml 2-propanol. After heating to 50 C under nitrogen for 1 hour, the solvent was removed and another 10 ml of 2-propanol were added and removed by distillation under reduced pressure. An oil was obtained which crystallized on standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09011734B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-5e889594c32f42beb10fcf1ccd4d2afc |
| Source note | uspto-grants-2015_04 |