HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetraethylammonium Hydroxide → HCID 66628108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetraethylammonium Hydroxide | HCID 6509 | — |
| Reactant | Diphenylphosphinic acid | HCID 15567 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 66628108 | HCID 66628108 | — |
Reaction Steps
To a flask were added 1.0 g diphenylphosphinic acid, 3.2 g of a 20% solution of tetraethylammonium hydroxide in water and 20 ml 2-propanol. After heating to 50 C under nitrogen for 1 hour, the solvent was removed and another 20 ml of 2-propanol were added and removed by distillation under reduced pressure. After drying, an oil was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09011734B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-e3cf61dd76684ec682b49365d32a30cf |
| Source note | uspto-grants-2015_04 |