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HRID1471800

反应详情

EQUATION

反应方程式

HRID 1471800 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OB(C2=CCN(S(C)(=O)=O)CC2)OC1(C)C
HCID67973497

未命名化合物

结构：CC(C)(C)OC(=O)N1CCC(C)(c2cc3cc(Cl)ncc3o2)CC1
HCID86694576

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCC(C)(c2cc3cc(C4=CCN(S(C)(=O)=O)CC4)ncc3o2)CC1
HCID86694587

未命名化合物

PROCEDURE

实验过程

The title compound is prepared from 4-(5-chloro-furo[2,3-c]pyridin-2-yl)-4-methyl-piperidine-1-carboxylic acid tert-butyl ester and 1-methanesulfonyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-1,2,3,6-tetrahydro-pyridine following a procedure analogous to that described for Example 1; the reaction is conducted at 150° C. LC (method 4): tR=1.58 min; Mass spectrum (ESI+): m/z=476 [M+H]+.

WORKUP

后处理

  1. customis conducted at 150° C