Acetic Acid → HCID 58070090, compound

Participants

Reaction Conditions

Reaction Steps

The Bromoacid 13 (2 mmol) is dissolved in 2M solution of dimethylamine in THF (20 mL) and to it 1 g of anhydrous K2CO3 was added and the mixture was heated in a pressure bottle at 50° C. overnight. The TLC showed the completion of the reaction. The reaction mixture was acidified with acetic acid and diluted with water (100 mL) and extracted with dichloromethane (2×60 mL). The combined organic layers were concentrated dried and used as such in the next reaction. MW calcd for C23H43NO6 429.59. Found 430.6 (MH)+.

Provenance & Evidence