HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroquinolin-6-ol → 4-(6-Hydroxyquinolin-2-yl)-3-methoxybenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroquinolin-6-ol | HCID 22132577 | — |
| Reactant | 4-Borono-3-methoxybenzoic acid | HCID 23134276 | — |
| Product | 4-(6-Hydroxyquinolin-2-yl)-3-methoxybenzoic acid | HCID 56961057 | — |
Reaction Steps
Followed Scheme 3: Starting Materials: 2-chloroquinolin-6-ol and 4-borono-3-methoxybenzoic acid. 1H NMR (CD3OD, 400 MHz): δ 8.81 (d, J=8.4 Hz, 1H), 8.14 (d, J=9.2 Hz, 1H), 8.10 (d, J=8.4 Hz, 1H), 7.89 (dd, J=6.8, 1.6 Hz, 2H), 7.85 (d, J=8.4 Hz, 1H), 7.69 (dd, J=9.2, 2.8 Hz, 1H), 7.48 (d, J=2.8 Hz, 1H). MS (ESI): m/z 295.7 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09012646B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-2e9a0969da0e4330a911db5a785034d1 |
| Source note | uspto-grants-2015_04 |