HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 68707573, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 59589531 | HCID 59589531 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68707573 | HCID 68707573 | — |
Reaction Steps
To a solution of N-[5-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-[1,2,4]triazolo[1,5-a]pyridin-2-yl]-acrylamide (0.05 g, 0.155 mmol) in ethanol (2 mL) was added N-methylpiperazine (0.13 g, 1.86 mmol) and the solution was stirred overnight. The reaction mixture was purified by prep LCMS. LCMS Method: 2, RT: 2.09 min, MI: 423 [M+1].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09012633B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-ba938ae3650d498d9aa26690befbf107 |
| Source note | uspto-grants-2015_04 |