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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1472810Generated: October 30, 2026

1-Methylpiperazine → HCID 68707573, compound

https://huagongshe.com/reaction/1472810

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-MethylpiperazineHCID 53167—
ReactantHCID 59589531HCID 59589531—
SolventEthanolHCID 702—
ProductHCID 68707573HCID 68707573—

Reaction Steps

To a solution of N-[5-(2,3-dihydro-benzo[1,4]dioxin-6-yl)-[1,2,4]triazolo[1,5-a]pyridin-2-yl]-acrylamide (0.05 g, 0.155 mmol) in ethanol (2 mL) was added N-methylpiperazine (0.13 g, 1.86 mmol) and the solution was stirred overnight. The reaction mixture was purified by prep LCMS. LCMS Method: 2, RT: 2.09 min, MI: 423 [M+1].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09012633B2
Source datasetuspto-grants-2015_04
ORD IDord-ba938ae3650d498d9aa26690befbf107
Source noteuspto-grants-2015_04