HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15434420, compound → Desfesoterodine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15434420 | HCID 15434420 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Desfesoterodine | HCID 9819382 | — |
Reaction Steps
(R)-[4-benzyloxy-3-(3-diisopropylamino-1-phenylpropyl)-phenyl]-methanol of formula (H) is reduced by using Pd/C in the presence of alcoholic solvents, preferably methanol to obtain (R)-2-(3-diisopropylamino-1-phenylpropyl)-4-hydroxy methyl phenol of formula (I) which is recrystallized with mixture of ethyl acetate and hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09012678B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-ba558b50854944408236d59f4f84c85b |
| Source note | uspto-grants-2015_04 |