HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Octyldodecanol → HCID 178514077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Octyldodecanol | HCID 21414 | — |
| Reactant | Isocyanate | HCID 105034 | — |
| Reactant | Di-n-butyldilauryltin | HCID 9809426 | — |
| Reactant | HCID 178514078 | HCID 178514078 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | 2-Methyltetrahydrofuran | HCID 7301 | — |
| Product | HCID 178514077 | HCID 178514077 | — |
Reaction Steps
70 g of ureidopyrimidone diisocyanate are dissolved in methyltetrahydrofuran, under argon. 80.3 g of octyldodecanol in 100 ml of dichloromethane are added, under argon, followed by addition of 15 microliters of dibutyltin dilaurate (catalyst). The reaction mixture is refluxed until the isocyanate peak (2250-2265 cm−1) has disappeared on IR spectrometry.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09017648B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-0d5f6ff408504497968ff69799eb29a5 |
| Source note | uspto-grants-2015_04 |