Lithium bis((trifluoromethyl)sulfonyl)azanide → HCID 131732761, compound

HRID 1473739Notes

Reaction equation

HRID 1473739 reaction equation
[CH3:1][NH:2][C:3](=[O:5])[O-:4].[Li+:6].[C:7]([S:11]([N-:14][S:15]([C:18]([F:21])([F:20])[F:19])(=[O:17])=[O:16])(=[O:13])=[O:12])([F:10])([F:9])[F:8]>>[CH3:1][NH:2][C:3](=[O:4])[O-:5].[Li+:6].[C:18]([S:15]([N-:14][S:11]([C:7]([F:10])([F:9])[F:8])(=[O:13])=[O:12])(=[O:16])=[O:17])([F:20])([F:19])[F:21]

Participants

3

Reactant 2

HCID 3816071Lithium bis((trifluoromethyl)sulfonyl)azanideHCID 21584661Npc184782

Product 1

HCID 131732761HCID 131732761, compoundYield 141.8%

Procedure

4.7 g of purified methylcarbamate and 6 g of LiTFSI were put into a round bottom flask and slowly stirred for 2 hours at room temperature under a nitrogen atmosphere, thereby yielding 10.7 g of a eutectic mixture.

Sources & evidence

ORD record
ord-cabea3a9901143a899597ed977d53fd2
Source dataset
uspto-grants-2015_04
Patent number
US09017881B2

Reaction notes

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