HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoylacetonitrile → HCID 178434323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoylacetonitrile | HCID 138308 | — |
| Reactant | HCID 178434325 | HCID 178434325 | — |
| Product | HCID 178434323 | HCID 178434323 | — |
Reaction Steps
Following the procedure described for Example 2A, the title compound was prepared using 500 mg (2.81 mmol) 6-fluoro-3-methyl-1H-indazole-5-carbaldehyde (Example 3A) and 566 mg (3.09 mmol) 3-(4-chlorophenyl)-3-oxopropanenitrile to yield 830 mg (66% of th.) of the crude product (76% purity) which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018234B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-cd03ffae62884aea9ce0b0eed8fed7ae |
| Source note | uspto-grants-2015_04 |