L-Phenylalanine → HCID 66787548, compound

Participants

Reaction Steps

5.03 g of phenylalanine and 22.8 g of 4-phenyl-1-butanol were added to 17 mL of 1,4-dioxane, 17 mL of 4N—HCl/1,4-dioxane was added thereto, and the reaction solution was stirred at room temperature for 4 days. The reaction solution was filtered and the filtrate was added with 450 mL of diethyl ether, and stirred at room temperature for 1.5 hours. The deposit was taken by filtration, washed with 50 mL of diethyl ether, and then dried under vacuum, thereby to give 5.90 g of Compound 16.

Provenance & Evidence