HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 5-bromo-N,N-dimethyl-2,3-dihydro-1H-indole-6-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 1-acetyl-5-bromo-2,3-dihydro-1H-indole-6-sulfonyl chloride | HCID 14024584 | — |
| Product | 5-bromo-N,N-dimethyl-2,3-dihydro-1H-indole-6-sulfonamide | HCID 70980687 | — |
Reaction Steps
Starting with dimethylamine and 1-acetyl-5-bromo-2,3-dihydro-1H-indole-6-sulfonyl chloride, the title compound was prepared by using similar methods to those described for Preparation 27.1H NMR (DMSO-d6): 7.40 (1H, s), 7.01 (1H, s), 3.51 (2H, t), 3.01 (2H, t), 2.77 (6H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018214B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-0038fe9784bb4dd794ef194bde350b58 |
| Source note | uspto-grants-2015_04 |