(3,5-Dichlorophenyl)hydrazine monohydrochloride → 4,6-Dichloro-3,3-dimethyl-2,3-dihydro-1H-indole

HRID 1475314Notes

Reaction equation

HRID 1475314 reaction equation
Cl.[Cl:2][C:3]1[CH:4]=[C:5]([NH:10]N)[CH:6]=[C:7]([Cl:9])[CH:8]=1.ClC1C=[C:20]2[C:16]([C:17](C)(C)CN2)=[CH:15]C=1>>[Cl:2][C:3]1[CH:8]=[C:7]([Cl:9])[CH:6]=[C:5]2[C:4]=1[C:16]([CH3:20])([CH3:17])[CH2:15][NH:10]2

Participants

3

Reactant 2

HCID 2723913(3,5-Dichlorophenyl)hydrazine monohydrochlorideHCID 204468746-chloro-3,3-dimethyl-2,3-dihydro-1H-indole

Product 1

HCID 812227034,6-Dichloro-3,3-dimethyl-2,3-dihydro-1H-indole

Procedure

Prepared from 3,5-dichlorophenylhydrazine hydrochloride in an analogous manner to that described for 6-chloro-3,3-dimethyl-2,3-dihydro-1H-indole (Preparation 25). MS: [M+H]+=216.

Sources & evidence

ORD record
ord-e8f371ad3e9a49c381a267567988e914
Source dataset
uspto-grants-2015_04
Patent number
US09018214B2

Reaction notes

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