HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N,N',N'-Tetramethylethylenediamine → HCID 70980241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N,N',N'-Tetramethylethylenediamine | HCID 8037 | — |
| Reactant | 6-Chloro-1,3-dihydroindol-2-one | HCID 736344 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 70980241 | HCID 70980241 | 23.2% |
Reaction Steps
Following similar methods to those described in Preparation 321 starting from 6-chloro-1,3-dihydro-indol-2-one (4 g, 25 mmol), TMEDA(11.2 mL, 79 mmol), BuLi (1.6M in hexane, 30 mL, 48 mmol) and Etl (2.9 mL, 36 mmol) gave the title compound (1.3 g). MS: [M+H]+=224.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018214B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-2741f44eeae245a2830d1db4fb0c8606 |
| Source note | uspto-grants-2015_04 |