4,4,5,5-Tetramethyl-2-(prop-1-en-2-yl)-1,3,2-dioxaborolane → HCID 86724036, compound

HRID 1475494Notes

Reaction equation

HRID 1475494 reaction equation
[C:1]([O:5][C:6]([N:8]1[C:16]2[CH:15]=[C:14](Cl)[N:13]=[CH:12][C:11]=2[C:10]([CH3:19])([CH3:18])[CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[C:20](B1OC(C)(C)C(C)(C)O1)([CH3:22])=[CH2:21]>>[C:1]([O:5][C:6]([N:8]1[C:16]2[CH:15]=[C:14]([C:20]([CH3:22])=[CH2:21])[N:13]=[CH:12][C:11]=2[C:10]([CH3:19])([CH3:18])[CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 109974264,4,5,5-Tetramethyl-2-(prop-1-en-2-yl)-1,3,2-dioxaborolaneHCID 86723969tert-Butyl 6-chloro-3,3-dimethyl-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

Product 1

HCID 86724036HCID 86724036, compound

Procedure

Prepared from 6-chloro-3,3-dimethyl-2,3-dihydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert butyl ester and 2-isopropenyl-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane using a procedure analogous to that of Preparation 379. MS: [M+H]+=289.

Workup

  1. customof Preparation 379

Sources & evidence

ORD record
ord-9ec27af654d9423d9c5198ff87048248
Source dataset
uspto-grants-2015_04
Patent number
US09018214B2

Reaction notes

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