Lithium methanolate → HCID 86665003, compound

Participants

Reaction Steps

Solution of 0.200 g (0.51 mmol) of titanium 2,4,5-tri-tert-butyl-imidazolate trichloride in 2 ml of d8-toluene was added to 0.08 g (2.11 mmol) of lithium methoxide at RT in a small vail inside nitrogen purged glove box. The slurry was agitated at RT for 16 hours and filtered. Solution analysis by 1H and 13C NMR indicated ˜78% conversion into titanium 2,4,5-tri-tert-butyl-imidazolatedichloride methoxide:

Provenance & Evidence