HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,4-Dichloropyrimidine → 3-(2-Chloro-pyrimidin-4-yl)-benzoic acid ethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,4-Dichloropyrimidine | HCID 77531 | — |
| Edukt | (3-Ethoxycarbonylphenyl)boronic acid | HCID 3249312 | — |
| Produkt | 3-(2-Chloro-pyrimidin-4-yl)-benzoic acid ethyl ester | HCID 24901959 | — |
Reaktionsschritte
2,4 dichloropyrimidine was coupled to 3-carboethoxyphenylboronic acid following procedure A. LC-MS showed the product to be >95% pure and to have the expected M+H+ of 195.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07732444B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-170816a7aa4a4582a5ce03540b74941a |
| Quellennotiz | uspto-grants-2010_06 |