Tetrahydrofuran → HCID 123498468, compound

Participants

Reaction Steps

An n-BuLi (3 mmol) hexane solution was added to a THF (10 ml) solution of naphtho[1,2-b:5,6-b′]dithiophene (1 mmol), and stirred at room temperature for one hour. This reaction mixture was slowly added with triisopropylsilyl chloride (4 mmol), and further, stirred at room temperature for 16 hours. Further, diluted with water (50 ml), and 1N hydrochloric acid (50 ml) was added. A precipitate formed was filtered out and washed with water, methanol, or hexane such that the compound A1 was obtained as a white solid.

Provenance & Evidence