HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 53241085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Benzofuran-2-sulfonyl chloride | HCID 2795172 | — |
| Reactant | (Acetyloxy)-carbamic acid tert-butyl ester | HCID 10058028 | — |
| Product | HCID 53241085 | HCID 53241085 | — |
Reaction Steps
N-[(tert-Butoxy)carbonyl]-1-benzofuran-2-sulfonamido acetate (56) is prepared from [(tert-butoxy)carbonyl]amino acetate, sodium hydride and 1-benzofuran-2-sulfonyl chloride according to Scheme 2. (3.1 g, 75%), 1H NMR (250 MHz, DMF) δ ppm 8.07 (1H, d, 0.9 Hz), 7.91 (1H, d, 7.3 Hz), 7.82 (1H, dd, 8.5, 0.8 Hz), 7.64 (1H, td, 7.8, 1.4 Hz), 7.41-7.52 (1H, m), 2.32 (3H, s), 1.37 (9H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018411B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-50c703b87d2944d8848242d78d5d920a |
| Source note | uspto-grants-2015_04 |