HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 53241083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | [(tert-Butoxy)carbonyl]amino 2,2-dimethylpropanoate | HCID 300008 | — |
| Reactant | 633305-21-2 | HCID 54346504 | — |
| Product | HCID 53241083 | HCID 53241083 | — |
Reaction Steps
N-[(tert-Butoxy)carbonyl]3-chlorothiophene-2-sulfonamido 2,2-dimethylpropanoate (107) is synthesised from 3-chlorothiophene-2-sulfonyl chloride, sodium hydride and [(tert-butoxy)carbonyl]amino 2,2-dimethylpropanoate according to Scheme 2. δH (500 MHz, DMSO-d6) 8.29 (1H, d, 5.3 Hz), 7.40 (1H, d, 5.2 Hz), 1.39 (9H, s), 1.28 (9H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018411B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-642fb9b464ce487ab30f221f3fa62279 |
| Source note | uspto-grants-2015_04 |