HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → HCID 20253494, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Phosphinic Acid | HCID 4124402 | — |
| Catalyst | 4,6-Bis(diphenylphosphino)phenoxazine | HCID 3255346 | — |
| Catalyst | (1E,4E)-1,5-diphenylpenta-1,4-dien-3-one; palladium | HCID 6505921 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20253494 | HCID 20253494 | 94.2% |
Reaction Steps
Example 1 is repeated with 99 g of phosphinic acid, 156 g of styrene, 8.7 mg of bis(dibenzylideneacetone)palladium and 5.7 mg of 4,6-bis(diphenylphosphino)-phenoxazine in 400 g of acetonitrile to obtain 240 g (94% of theory) of 2-phenyl-ethylphosphonous acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018413B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-36efe554c4ba43e1bddce302c6096631 |
| Source note | uspto-grants-2015_04 |