HCID 58288210, compound → HCID 58288224, compound

Participants

Reaction Steps

135 mg (0.29 mmol) of tert-butyl {1-[4-chloro-3-(dibenzylamino)phenyl]cyclopropyl}acetate were dissolved in 10 ml of ethyl acetate, 15 mg of palladium on carbon (10%) were added and the mixture was stirred at RT under an atmosphere of hydrogen at atmospheric pressure for 2 h. The reaction mixture was then filtered off through celite, the residue was washed with ethyl acetate and the filtrate was concentrated. This gave 73 mg of the title compound (89% of theory).

Provenance & Evidence