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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1476610Generated: October 31, 2026

Trifluoroacetic acid → HCID 67259075, compound

https://huagongshe.com/reaction/1476610

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 67258405HCID 67258405—
SolventDichloromethaneHCID 6344—
ProductHCID 67259075HCID 67259075—

Reaction Steps

A solution of tert-butyl 4-{1-[(2-ethyl-2H-1,2,3-triazol-4-yl)methyl]-2,4-dioxo-6-phenyl-1,4-dihydrothieno[3,2-d]pyrimidin-3(2H)-yl}piperidine-1-carboxylate (2.10 g; compound B21) in DCM (50 ml) is reacted with trifluoroacetic acid (10 ml) according to the procedure described in example B43 to afford the title compound as a solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09018175B2
Source datasetuspto-grants-2015_04
ORD IDord-d29b84cc97264cd08cde852cf6e50379
Source noteuspto-grants-2015_04