HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67258440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67259055 | HCID 67259055 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67258440 | HCID 67258440 | — |
Reaction Steps
A solution of tert-butyl 4-{1-[(3-ethyl-1,2,4-thiadiazol-5-yl)methyl]-2,4-dioxo-6-phenyl-1,4-dihydrothieno[3,2-d]pyrimidin-3(2H)-yl}piperidine-1-carboxylate (321 mg; compound B22) in DCM (10 ml) is reacted with trifluoroacetic acid (2 ml) according to the procedure described in example B43 to afford the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018175B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-89e6a8598629451e904da1f5294e1751 |
| Source note | uspto-grants-2015_04 |