HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67259261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67258349 | HCID 67258349 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67259261 | HCID 67259261 | — |
Reaction Steps
According to the procedure described for compound B92 tert-butyl 4-{1-[(5-ethylthiophen-2-yl)methyl]-2,4-dioxo-6-phenyl-1,4-dihydrothieno[3,2-d]pyrimidin-3(2H)-yl}piperidine-1-carboxylate (1.18 g, compound B73) and a solution of hydrogen chloride in 1,4-dioxane (8.0 ml, 6.8 M) are reacted in 1,4-dioxane (35 ml) to afford the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09018175B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-b32fe819d9ab4a72a3c1fab079578903 |
| Source note | uspto-grants-2015_04 |