HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide | HCID 71811587 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide hydrochloride | HCID 118386969 | 94.2% |
Reaction Steps
2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide dissolved in EA, stirred at room temperature, while HCl is inlet till occurred to white solid. The reaction mixture was filtered to get White solid; 94.2% yield;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09402819B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-81815eb3c1d54bb1b2ab89da27304eb8 |
| Source note | uspto-grants-2016_08 |