HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 178463807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 178424455 | HCID 178424455 | — |
| Product | HCID 178463807 | HCID 178463807 | — |
Reaction Steps
The title compound is prepared from 4-cyano-1H-imidazole-2-carboxylic acid [2-(4,4-dimethyl-cyclohex-1-enyl)-4-(4-oxo-cyclohexyl)-phenyl]-amide (as prepared in Example 23) and diethylamine using NaBH(OAc)3 according to literature procedure (J. Org. Chem., 61, 3849-62 (1996)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403804B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-f2adaa806e474bee88f29404ae2008f4 |
| Source note | uspto-grants-2016_08 |