HRID1477695

反应详情

EQUATION

反应方程式

HRID 1477695 的结构方程式

PROCEDURE

实验过程

The synthesis was performed using 4-[4-(2,4-difluorophenyl)piperazin-1-yl]-1,3,5-triazin-2(1H)-one (189 mg, 0.65 mmol) synthesized in Reference Synthesis Example 86 and [3-(trifluoromethyl)-1H-pyrazol-1-yl]methyl 4-methylbenzenesulfonate (413 mg, 1.29 mmol) synthesized in Reference Synthesis Example 15 in a similar manner to Synthesis Example 1 to obtain the title compound (21 mg, yield: 7.4%).

WORKUP

后处理

  1. customsynthesized in Reference Synthesis Example 15 in a similar manner to Synthesis Example 1