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HRID1477802

反应详情

EQUATION

反应方程式

HRID 1477802 的结构方程式

REACTANTS

反应物

2
结构：CC(C)[C@@](C)(N)CO
HCID12113027

未命名化合物

结构：O=C(O)c1cnc(C2CC2)c(OCC2CC2)n1
HCID86682331

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)[C@](C)(CO)NC(=O)c1cnc(C2CC2)c(OCC2CC2)n1
HCID71526036

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized in analogy to Example 15, using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g; 100 mg, 0.42 mmol) and (2R)-2-amino-2,3-dimethyl-1-butanol (CAN 155158-75-1, 107.06 mg, 0.64 mmol) as starting materials, and isolated (20 mg, 14.04%) as off white sticky solid, LC-MS (UV peak area, ESI) 100%, 334.4 (M+H).

WORKUP

后处理

  1. customisolated (20 mg, 14.04%) as off white sticky solid, LC-MS (UV peak area, ESI) 100%, 334.4 (M+H)