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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1477933Generated: October 30, 2026

HCID 86705063, compound → HCID 70561537, compound

https://huagongshe.com/reaction/1477933

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86705063HCID 86705063—
CatalystNickelHCID 935—
SolventMethanolHCID 887—
ProductHCID 70561537HCID 70561537—

Reaction Steps

A mixture of the product from Step A (68 mg, 0.162 mmol) and Raney-Ni (1 mg) in MeOH (10 mL) was purged air three times and then backfilled with H2. The mixture was stirred at ambient temperature overnight. The suspension was filtered off and the filtrate was concentrated to afford the title compound as a colorless solid. LC/MS m/z=406.0 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09403807B2
Source datasetuspto-grants-2016_08
ORD IDord-a978614e271947cbace0b1b3f65e371c
Source noteuspto-grants-2016_08