HCID 90238651, compound → HCID 90238531, compound

HRID 1478773Notes

Reaction equation

HRID 1478773 reaction equation
C([O:3][CH:4](OCC)[CH2:5][O:6][C@@H:7]([C@@H:11]1[CH2:15][CH2:14][CH2:13][O:12]1)[CH2:8][CH:9]=[CH2:10])C.C[C@@H]1C[C@H]1C(OCC=O)CC=C>>[O:12]1[CH2:13][CH2:14][CH2:15][C@H:11]1[C@H:7]([O:6][CH2:5][CH:4]=[O:3])[CH2:8][CH:9]=[CH2:10]

Participants

3

Reactant 2

HCID 90238651HCID 90238651, compoundHCID 90253550HCID 90253550, compound

Product 1

HCID 90238531HCID 90238531, compound

Procedure

(2S)-2-[(1R)-1-(2,2-Diethoxyethoxyl)but-3-en-1-yl]tetrahydrofuran (C95) was converted to the product using the method described for the synthesis of ({1-[(1R,2R)-2-methylcyclopropyl]but-3-en-1-yl}oxy)acetaldehyde (C83) in Example 20. The resulting product was used in the next step without further purification. Yield: 6 g, ≦33 mmol, ≦35%.

Workup

  1. customThe resulting product was used in the next step without further purification

Sources & evidence

ORD record
ord-59e1b4f77223437e9da5bddae08a97db
Source dataset
uspto-grants-2016_08
Patent number
US09403846B2

Reaction notes

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