HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl methyl ether → 1-(4-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl methyl ether | HCID 15413 | — |
| Reactant | Benzene, 1-azido-4-chloro- | HCID 76803 | — |
| Reactant | HCID 118513266 | HCID 118513266 | — |
| Product | 1-(4-chlorophenyl)-5-methyl-1H-1,2,3-triazole-4-carboxylic acid | HCID 4979941 | — |
Reaction Steps
The title compound was prepared analogously to 1-(2-chloro-4-methoxyphenyl)-5-methyl-1H-1,2,3-triazole-4-carboxylic acid (Example 1 step 2) by replacing 1-azido-2-chloro-4-methoxybenzene with 1-azido-4-chlorobenzene in (0.5 M in TBME).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403833B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-d06b40b8d36c4368a7d029b8d9c3ded8 |
| Source note | uspto-grants-2016_08 |