HCID 57702611, compound → Naphthalene

Participants

Reaction Steps

Preparation analogous to Example 3b. Instead of 19.5 g (40 mmol) of 9,10-bis(2-bromophenyl)anthracene, 25.5 g (40 mmol) of 1,4-bis(10-bromoanthracen-9-yl)naphthalene are used. Sublimation at p=1×10−5 mbar, T=300° C. Yield: 12.1 g (16.5 mmol), 41.3% of theory; purity: 99.8% according to 1H-NMR.

Provenance & Evidence