HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 90203560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Fluoropropan-2-ol | HCID 101671 | — |
| Reactant | 3-Bromo-4-chloropyridine | HCID 817696 | — |
| Product | HCID 90203560 | HCID 90203560 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 108b, using 3-bromo-4-chloropyridine (CAN 36953-42-1), 1-fluoropropan-2-ol (CAN 430-50-2) as starting materials and sodium hydride as reagent. The title compound was isolated (7.55 g, 62%) as a yellow oil; MS (ESI, m/z): 235.9 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409866B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-ffb695f3a61c46c8958c9a1240906c37 |
| Source note | uspto-grants-2016_08 |