HCID 178422047, compound → HCID 178422052, compound

HRID 1480526Notes

Reaction equation

ClC1C=C2C(C)(C)/C(=C\C=C(/C3C=CC=C(CCCCC(O[N:70]4[C:74](=[O:75])[CH2:73][CH2:72][C:71]4=[O:76])=O)C=3)\C=C\C3C(C)(C)C4C5C=C(S([O-])(=O)=O)C=C(S([O-])(=O)=O)C=5C=CC=4[N+]=3CCCCS([O-])(=O)=O)/N=C2N(CCCCS([O-])(=O)=O)C=1.[Na+:77].[Na+].[Na+].[C:80]([CH2:83][CH2:84][CH2:85][CH2:86][C:87]1[CH:88]=[C:89](/[C:93](=[CH:119]\[CH:120]=[C:121]2/[C:122]([CH3:140])([CH3:139])[C:123]3[C:124](=[N:138]/2)[N:125]([CH2:130][CH2:131][CH2:132][CH2:133][S:134]([O-:137])(=[O:136])=[O:135])[CH:126]=[C:127]([Cl:129])[CH:128]=3)/[CH:94]=[CH:95]/[C:96]2[C:104]([CH3:106])([CH3:105])[C:103]3[C:98](=[CH:99][CH:100]=[C:101]([S:107]([O-:110])(=[O:109])=[O:108])[CH:102]=3)[N+:97]=2[CH2:111][CH2:112][CH2:113][CH2:114][S:115]([O-:118])(=[O:117])=[O:116])[CH:90]=[CH:91][CH:92]=1)([OH:82])=[O:81].[Na+].[Na+]>>[Cl:129][C:127]1[CH:128]=[C:123]2[C:122]([CH3:140])([CH3:139])/[C:121](=[CH:120]\[CH:119]=[C:93](/[C:89]3[CH:90]=[CH:91][CH:92]=[C:87]([CH2:86][CH2:85][CH2:84][CH2:83][C:80]([O:82][N:70]4[C:74](=[O:75])[CH2:73][CH2:72][C:71]4=[O:76])=[O:81])[CH:88]=3)\[CH:94]=[CH:95]\[C:96]3[C:104]([CH3:105])([CH3:106])[C:103]4[C:98](=[CH:99][CH:100]=[C:101]([S:107]([O-:110])(=[O:108])=[O:109])[CH:102]=4)[N+:97]=3[CH2:111][CH2:112][CH2:113][CH2:114][S:115]([O-:118])(=[O:116])=[O:117])/[N:138]=[C:124]2[N:125]([CH2:130][CH2:131][CH2:132][CH2:133][S:134]([O-:137])(=[O:136])=[O:135])[CH:126]=1.[Na+:77].[Na+:77]

Participants

Reactant 2

HCID 178422047HCID 178422047, compound

HCID 178422051HCID 178422051, compound

Product 1

HCID 178422052HCID 178422052, compound

Procedure

Compound 50 is prepared analogously to compound 29 (Example 38), except that compound 49 is used as a starting material.

Sources & evidence

ORD record: ord-c772981a49f649e3afb364c008bf84a3
Source dataset: uspto-grants-2016_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09408924B2

Reaction notes

Loading…