HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89996011, compound → HCID 73386781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89996011 | HCID 89996011 | — |
| Reactant | HCID 89996023 | HCID 89996023 | — |
| Product | HCID 73386781 | HCID 73386781 | 21% |
Reaction Steps
The title compound was prepared according to Example 40 using N-(4-(1,3-dimethyl-1H-pyrazol-4-yl)-2-methoxyphenyl)formamide (Preparation 76) and 2-(methylsulfonyl)-N-neopentylpyrido[3,4-d]pyrimidin-8-amine (Preparation 47). The residue was purified by silica gel column chromatography eluting with 50-100% EtOAc in cyclohexane to give the title compound (4 mg, 21%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409907B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-5d71bbaf3e584107b944b8f2878f5d80 |
| Source note | uspto-grants-2016_08 |