HRID1480849

反应详情

EQUATION

反应方程式

HRID 1480849 的结构方程式

PROCEDURE

实验过程

The title compound was prepared according to the method described for Preparation 158 using (4-bromo-1-methyl-1H-pyrazol-5-yl)methanol (Preparation 222) and 2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline. The residue was purified using Biotage silica gel column chromatography eluting with EtOAc followed by elution through an SCX-2 cartridge.

WORKUP

后处理

  1. customThe residue was purified
  2. washeluting with EtOAc
  3. washfollowed by elution through an SCX-2 cartridge