HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → 1-(3-Methoxy-4-nitrophenyl)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 5-Fluoro-2-nitroanisole | HCID 2779250 | — |
| Product | 1-(3-Methoxy-4-nitrophenyl)piperidine | HCID 2867534 | — |
Reaction Steps
The title compound was prepared according to the method described for Preparation 78 using 4-fluoro-2-methoxy-1-nitrobenzene and piperidine. The residue was purified using silica gel column chromatography eluting with 50-80% DCM in cyclohexanes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409907B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-40945690c574464180382aebfe76247c |
| Source note | uspto-grants-2016_08 |