2-Butene-1,4-diol, (2Z)- → HCID 14722758, compound

HRID 1481638Notes

Reaction equation

HRID 1481638 reaction equation
C(O)/C=C\CO.[C:7]([O:11][C:12]([NH:14][CH2:15][C:16]#[C:17][CH2:18][OH:19])=[O:13])([CH3:10])([CH3:9])[CH3:8]>>[C:7]([O:11][C:12]([NH:14][CH2:15]/[CH:16]=[CH:17]\[CH2:18][OH:19])=[O:13])([CH3:10])([CH3:9])[CH3:8]

Participants

3

Reactant 2

HCID 6437902-Butene-1,4-diol, (2Z)-HCID 23818252HCID 23818252, compound

Product 1

HCID 14722758HCID 14722758, compoundYield 30%

Procedure

The title compound was synthesized from cis-2-butene-1,4-diol in an overall yield of 30% according to the procedure used for 4-tert-butoxycarbonylamino-2-butyn-1-ol.

Sources & evidence

ORD record
ord-854215ef757244ad832b128d9932bba0
Source dataset
uspto-grants-2016_08
Patent number
US09409945B2

Reaction notes

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