Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Reactant | HCID 59174704 | HCID 59174704 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 59174619 | HCID 59174619 | 27.4% |
Reaction Steps
The 2-methylsulfone of 7 (1.0 g, 1.9 mmol) was mixed with 3-methoxyaniline (420 mg, 3.4 mmol) in DMA and the mixture was heated at 90° C. for 24 hours. Workup was done in a manner similar to that for Step-5 in Example 57 to give 9 (300 mg, 0.52 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09409921B2 |
|---|
| Source dataset | uspto-grants-2016_08 |
|---|
| ORD ID | ord-006aa6db3c684bfb91733755b858bcca |
|---|
| Source note | uspto-grants-2016_08 |
|---|
